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beyond the crack tip, the embedded subsurface cracks formed in the phase contrast image are roughly 2–3 μm wide. cross-sections of these surfaces indicate that the crack is continuous within the subsurface. this result demonstrates that the crack tip may be propagating a single mode crack, although this does not preclude the crack tip from being in the vicinity of two or more equivalent plastic modes ¹² . since the applied stress did not exceed the critical stress intensity factor of the igscc material, the stress corrosion cracks have been initiated by the dynamic tensile cracking of the internal oxide at the crack tip, and they propagate at some length from this position. comparing all the measurements carried out (morphology, chemistry, and stress analysis), this crack tip indeed forms within the active crack front.

the crack chemistry of the shear crack samples, measured using apt, suggest that the surface oxide is the direct crack locus. after fib milling, and sem inspection, this was validated by edx analysis. a series of images were taken across the crack in the direction of crack propagation, illustrating the oxidation of the crack front as it propagates into the subsurface, which corresponds to the image of fig. 4b. in this case, the crack tip has propagated 2 μm, but the same technique may be applied to even shorter cracks if needed.

furthermore, a complete analysis of the active crack front was made using cross-sectional and surface cuts. this was performed using a combination of surface shear measurements and analysis of indentations, performed using hs-afm. hs-afm observation indicates that the high-resolution tip can be used to measure localised changes in shear modulus within the crack tip region. the experimentally determined profile of the crack front is then compared to the analytical representation obtained from a finite element model. this analysis demonstrates the ability of hs-afm to determine the crack tip geometry in both the surface and subsurface with a high degree of accuracy. in this case, a crack tip of 2 μm in length was modelled, and the estimates of the crack tip position and geometry showed good agreement with experiment. both the tip and the simulation show that crack tip is well-defined, and is equivalent to a circle with a radius of 1.5 μm. this result is similar to the igscc crack tip width reported previously in the literature, and is measured from a rounded corner tip ^{13, 14} .

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